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友田 陽*; 小嶋 真由美*; Harjo, S.; Gong, W.*; 佐藤 成男*; Ung
r, T.*
Materials Science & Engineering A, 743, p.32 - 39, 2019/01
被引用回数：25 パーセンタイル：81.14(Nanoscience & Nanotechnology)Heterogeneous plastic deformation behavior of 
oriented individual grains-family with respect to the tensile direction in austenitic steels was studied using electron back scatter diffraction (EBSD) and neutron diffraction (ND) measurements. The kernel averaged misorientation value determined by EBSD for a plastically deformed specimen was different in grain to grain, suggesting different dislocation densities. Such insights obtained from the surface observations with EBSD were quantitatively evaluated as bulk-averaged data using ND. The convolutional multiple whole profile fitting (CMWP) for ND profiles has revealed different dislocation densities in oriented grains-families, showing good coincidence with the EBSD results in trend.
neutron diffraction line profile analysisHarjo, S.; 川崎 卓郎; 友田 陽*; Gong, W.*; 相澤 一也; Tichy, G.*; Shi, Z.*; Ungr, T.*
Metallurgical and Materials Transactions A, 48(9), p.4080 - 4092, 2017/09
被引用回数：54 パーセンタイル：90.48(Materials Science, Multidisciplinary) neutron diffraction during tensile deformation of lath martensite steel containing 0.22 mass% of carbon, is performed using TAKUMI of J-PARC. The diffraction peaks at plastically deformed states exhibit asymmetries as the reflection of redistributions of the stress and dislocation densities/arrangements in lath-packets where the dislocation glides are favorable (soft packet) and unfavorable (hard packet). The dislocation density is as high as 10
m
at the as-quenched state, and then during tensile straining, the load and the dislocation density become different between the two lath-packets. The dislocation character and arrangement vary also in the hard packet, but hardly change in the soft packet. The hard packet plays an important role in the high work hardening in martensite, which could be understood by taking into account not only the increase of the dislocation density but also the change in dislocation arrangement.
Ungr, T.*; Harjo, S.; 川崎 卓郎; 友田 陽*; Ribrik, G.*; Shi, Z.*
Metallurgical and Materials Transactions A, 48(1), p.159 - 167, 2017/01
被引用回数：50 パーセンタイル：90.14(Materials Science, Multidisciplinary)Based on high-resolution neutron diffraction experiments we will show that in lath martensite steels the initially homogeneous dislocation structure is disrupted by plastic deformation, to produce a composite on the length scale of martensite lath packets. The diffraction patterns of plastically strained martensitic steel reveal characteristically asymmetric peak profiles in the same way as has been observed in materials with heterogeneous dislocation structures. Lath packets oriented favorably or unfavorably for dislocation glide become soft or hard. The lath packet type develops by work softening or work hardening in which the dislocation density becomes smaller or larger compared to the initial average one. The decomposition into soft and hard lath packets is accompanied by load redistribution between the two lath packet types. The composite behavior of plastically deformed lath martensite opens a new way to understand the elastic-plastic response in this class of materials.
neutron diffraction experiment川崎 卓郎; Harjo, S.; Gong, W.; 相澤 一也; 岩橋 孝明; Shi, Z.*; Li, J.*; 友田 陽*; Ungr, T.*
JPS Conference Proceedings (Internet), 8, p.031009_1 - 031009_5, 2015/09
鉄鋼材料に代表される金属材料の力学的特性を理解するためには、弾性ひずみだけでなく、転位の密度や配列状態など微細構造を評価することが重要である。これらの情報はX線や中性子回折パターンに表れるBraggピークの形状を詳しく解析することで得ることができる。透過能の高い中性子を用いることでバルク状態の材料内部の微細構造に関する情報を得ることができるが、これまで中性子(特にパルス中性子)はあまり適用されてこなかった。我々はJ-PARC物質生命科学実験施設BL19に設置された工学材料回折装置 匠を用いてマルテンサイト鋼の引張り試験その場中性子回折測定を行い、CMWP法と呼ばれる解析法を用いてこの材料の微細構造を調べた。その結果、巨視的なひずみの増加に伴う転位密度の増加は比較的小さく、転位配列の顕著な規則化が観測された。
